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1 article(s) from Crestey, François

A strategic approach to [6,6]-bicyclic lactones: application towards the CD fragment of DHβE

Tue Heesgaard Jepsen,
Emil Glibstrup,
François Crestey,
Anders A. Jensen and
Jesper Langgaard Kristensen

Beilstein J. Org. Chem. 2017, 13, 988–994, doi:10.3762/bjoc.13.98

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Figure 1: DHβE and related structures. The K_i values of the compounds at the rat α4β2 nAChR subtype determine...

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Scheme 1: First strategy towards the CD fragment (Ts-strategy). i) TsCl, TEA, DCM, 0 °C. ii) NaH, DMF, 0 °C, ...

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Scheme 2: First strategy towards the CD fragment (Cbz-strategy). i) R-Cl, TEA, CH₂Cl₂, 0 °C. ii) NaH, DMF, 0 ...

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Scheme 3: Second strategy towards the CD fragment. i) 4-Bromobut-1-ene, K₂CO₃, acetone, 70 °C. ii) n-BuLi, TH...

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Figure 2: The binding affinities of compounds 9 and 26 at the rat α4β2 nAChR. a) The AB fragment was evaluate...

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Published 22 May 2017

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